Methyl iodide → HCID 19075299, compound

HRID 257023Notes

Reaction equation

HRID 257023 reaction equation
[CH3:1][I:2].[CH2:3]([S:9][C:10]1[C:11]([C:15]2[CH:16]=[N:17][CH:18]=[CH:19][CH:20]=2)=[N:12][S:13][N:14]=1)[CH2:4][CH2:5][CH2:6][CH2:7][CH3:8]>>[I-:2].[CH2:3]([S:9][C:10]1[C:11]([C:15]2[CH:16]=[N+:17]([CH3:1])[CH:18]=[CH:19][CH:20]=2)=[N:12][S:13][N:14]=1)[CH2:4][CH2:5][CH2:6][CH2:7][CH3:8]

Participants

3

Reactant 2

HCID 6328Methyl iodideHCID 10755149HCID 10755149, compound

Product 1

HCID 19075299HCID 19075299, compound

Procedure

Methyl iodide (1 ml, 15 mmol) was added to a solution of 3-(4-hexylthio-1,2,5-thiadiazol-3-yl)pyridine (3 mmol) and the reaction mixture was stirred at room temperature for 48 h and evaporated.

Workup

  1. customevaporated

Sources & evidence

ORD record
ord-42346759dd284cd6b7cfa7c3c1a99ec9
Source dataset
uspto-grants-1993_11
Patent number
US05260311

Reaction notes

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