HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-methyl-4-nitrophenethylamine → 1-(4-nitrophenyl)-4-(N-methyl-N-(2-(4-nitrophenyl)ethyl)amino)piperidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-methyl-4-nitrophenethylamine | HCID 2794239 | — |
| Reactant | 1-(4-Nitrophenyl)piperidin-4-one | HCID 3842562 | — |
| Product | 1-(4-nitrophenyl)-4-(N-methyl-N-(2-(4-nitrophenyl)ethyl)amino)piperidine | HCID 19784394 | 52.5% |
Reaction Steps
2.4 g (10.9 mmol) of 1-(4-nitrophenyl)-4-piperidone and 2.0 g (10.9 mmol) of N-methyl-N-(2-(4-nitrophenyl)ethyl)amine were reacted in a similar manner to Example 1. 2.2 g of 1-(4-nitrophenyl)-4-(N-methyl-N-(2-(4-nitrophenyl)ethyl)amino)piperidine were obtained. Melting point 97°-98° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05260318 |
| Source dataset | uspto-grants-1993_11 |
| ORD ID | ord-c87b100564df46948eb0fbf4be09245b |
| Source note | uspto-grants-1993_11 |