HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl mercaptan → HCID 13581600, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl mercaptan | HCID 7509 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Benzene, 2-chloro-1,5-dinitro-3-(trifluoromethyl)- | HCID 67851 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 13581600 | HCID 13581600 | — |
Reaction Conditions
| Temperature | 0 °C |
|---|
Reaction Steps
67.6 g of 2-chloro-3,5-dinitrobenzotrifluoride are dissolved in 150 ml of N,N-dimethylformamide (DMF) and the mixture is treated with 35.9 g of solid potassium carbonate, treated dropwise with 31 g of benzylmercaptan in 200 ml of DMF with stirring at 0° C., and subsequently stirred for a further 16 hours at room temperature, while cooling.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05260423 |
| Source dataset | uspto-grants-1993_11 |
| ORD ID | ord-d6b8c35d48a6424c99ef491dfd6d32b1 |
| Source note | uspto-grants-1993_11 |