HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 15679401, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 13345321 | HCID 13345321 | — |
| Product | HCID 15679401 | HCID 15679401 | — |
Reaction Steps
48.9 g of 6-methylpyridine-2,3-dicarboxylic anhydride in 200 ml of methanol are refluxed for 3 hours while stirring. Evaporating down the mixture under reduced pressure gives 57.9 g of the title compound of melting point 133°-158° C. (decomposition).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05262387 |
| Source dataset | uspto-grants-1993_11 |
| ORD ID | ord-933a5e0476064b5fae2597e896712366 |
| Source note | uspto-grants-1993_11 |