O-ethylhydroxylamine hydrochloride → HCID 73473545, compound

HRID 257450Notes

Reaction equation

HRID 257450 reaction equation
[C:1]([OH:6])(=[O:5])[C:2]([OH:4])=[O:3].[CH2:7]([O:9][N:10]=[CH:11][C:12]1[CH:13]2[N:19]([CH3:20])[CH:16]([CH2:17][CH:18]=1)[CH2:15][CH2:14]2)C.C(C1C2N(C)C(CC=1)CC2)=O.Cl.C(ON)C>>[C:1]([OH:6])(=[O:5])[C:2]([OH:4])=[O:3].[CH3:7][O:9][N:10]=[CH:11][C:12]1[CH:13]2[N:19]([CH3:20])[CH:16]([CH2:17][CH:18]=1)[CH2:15][CH2:14]2

Participants

4

Reactant 3

HCID 76850O-ethylhydroxylamine hydrochlorideHCID 18960840HCID 18960840, compoundHCID 73473548HCID 73473548, compound

Product 1

HCID 73473545HCID 73473545, compound

Procedure

2-Ethoxyiminomethyl-8-methyl-8-azabicyclo[3.2.1]oct-2-ene oxalate from 2-formyl-8-methyl-8-azabicyclo[3.2.1]oct-2-ene and ethoxyamine hydrochloride. M.p. 127°-128° C.

Sources & evidence

ORD record
ord-b6a904dce5cf43dbb5e20b9cd84faff8
Source dataset
uspto-grants-1993_11
Patent number
US05262427

Reaction notes

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