4-Ethylpyridine → HCID 19783354, compound

HRID 257462Notes

Reaction equation

HRID 257462 reaction equation
[CH2:1]([C:3]1[CH:8]=[CH:7][N:6]=[CH:5][CH:4]=1)[CH3:2].[Cl:9][C:10]1[CH:18]=[CH:17][C:13]([CH2:14][CH2:15]Br)=[CH:12][CH:11]=1>>[Cl:9][C:10]1[CH:18]=[CH:17][C:13]([CH2:14][CH2:15][CH:1]([C:3]2[CH:8]=[CH:7][N:6]=[CH:5][CH:4]=2)[CH3:2])=[CH:12][CH:11]=1

Participants

3

Reactant 2

HCID 108224-EthylpyridineHCID 230291-(2-Bromoethyl)-4-chlorobenzene

Product 1

HCID 19783354HCID 19783354, compoundYield 59.8%

Procedure

1.0 g (9.35 mmol) of 4-ethylpyridine and 2.05 g (9.35 mmol) of 4-chlorophenethyl bromide were reacted in the same manner as in Example 1. The reaction product was purified to obtain 1.37 g of the desired compound (yield: 59.8%).

Workup

  1. customThe reaction product was purified

Sources & evidence

ORD record
ord-9d1fb33e8f904080a012e9db144921c8
Source dataset
uspto-grants-1993_11
Patent number
US05262420

Reaction notes

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