HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoethane → 1-Phenyl-3-(3-n-propyl-4-pyridyl)butane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | 1-Phenyl-3-(3-methyl-4-pyridyl)butane | HCID 19783297 | — |
| Reactant | Lithium diisopropylamine | HCID 45051747 | — |
| Product | 1-Phenyl-3-(3-n-propyl-4-pyridyl)butane | HCID 19783320 | 15.6% |
Reaction Steps
2.1 g (9.35 mmol) of 1-phenyl-3-(3-methyl-4-pyridyl)butane, 1.46 g (9.35 mmol) of ethyl iodide and 2 equivalent of lithium-diisopropylamine were reacted in the same manner as in Example 1. The reaction product was purified to obtain 0.37 g of the desired compound (yield: 15.6%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05262420 |
| Source dataset | uspto-grants-1993_11 |
| ORD ID | ord-050c0500979a4433a4718a4be18e859c |
| Source note | uspto-grants-1993_11 |