HCID 54081790, compound → HCID 14883838, compound

HRID 257495Notes

Reaction equation

HRID 257495 reaction equation
[CH2:1]([C:3]1[CH:4]=[N:5][CH:6]=[CH:7][C:8]=1[CH:9]=[C:10]([CH3:19])[CH2:11][CH2:12][C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)[CH3:2].C1(C=C(C)CC(C2C=CN=CC=2CC)C)C=CC=CC=1>>[CH2:1]([C:3]1[CH:4]=[N:5][CH:6]=[CH:7][C:8]=1[CH2:9][CH:10]([CH3:19])[CH2:11][CH2:12][C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)[CH3:2]

Participants

3

Reactant 2

HCID 54081790HCID 54081790, compoundHCID 54367985HCID 54367985, compound2×

Product 1

HCID 14883838HCID 14883838, compoundYield 78.5%

Procedure

The procedure of Example 50 was repeated with the exception that 1.2 g of 1-(3-ethyl-4-pyridyl)-2-methyl-4-phenyl-1-butene (compound 55) obtained in Example 42 was used in place of 1-phenyl-2-methyl-4-(3-ethyl-4-pyridyl)-1-pentene in Example 50, to obtain 0.95 g (yield: 78.4%) of 1-(3-ethyl-4-pyridyl)-2-methyl-4-phenylbutane (hereinafter referred to as compound 100).

Workup

  1. customobtained in Example 42

Sources & evidence

ORD record
ord-de8bfb9861c345dbac6f20d401451e41
Source dataset
uspto-grants-1993_11
Patent number
US05262420

Reaction notes

Loading…