Thionyl Chloride → HCID 54398879, compound

HRID 257578Notes

Reaction equation

HRID 257578 reaction equation
[Br:1][C:2]1[CH:22]=[CH:21][C:5]([CH2:6][CH:7]([C:15](=[O:20])[CH2:16][CH2:17][CH2:18][CH3:19])[C:8](=[N:12][O:13][CH3:14])[C:9](O)=[O:10])=[C:4]([F:23])[CH:3]=1.S(Cl)([Cl:26])=O>>[Br:1][C:2]1[CH:22]=[CH:21][C:5]([CH2:6][CH:7]([C:15](=[O:20])[CH2:16][CH2:17][CH2:18][CH3:19])[C:8](=[N:12][O:13][CH3:14])[C:9]([Cl:26])=[O:10])=[C:4]([F:23])[CH:3]=1

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 54146744HCID 54146744, compound

Product 1

HCID 54398879HCID 54398879, compound

Procedure

The title compound is prepared by reaction of 3-(4-bromo-2-fluorobenzyl)-2-methoxyimino-4-oxooctanoic acid (from Step F) with thionyl chloride according to the procedure of Example 4, Step D. The material is used without purification in the next step.

Workup

  1. customThe material is used without purification in the next step

Sources & evidence

ORD record
ord-d3d5eb4c03bd4e6485d63b0707f23a39
Source dataset
uspto-grants-1993_11
Patent number
US05262412

Reaction notes

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