HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyldioxirane → 1-Hydroxy-2,6-diphenyl-3-methylpiperidin-4-yl Laurate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyldioxirane | HCID 115197 | — |
| Reactant | 2,6-Diphenyl-3-methylpiperidin-4-yl Laurate | HCID 54052528 | — |
| Product | 1-Hydroxy-2,6-diphenyl-3-methylpiperidin-4-yl Laurate | HCID 54551106 | 99.4% |
Reaction Steps
The general procedure of Example 2 is repeated using 11.5 g (25.5 mmol) of 2,6-diphenyl-3-methylpiperidin-4-yl laurate and 570 mL (25.5 mmol) of dimethyldioxirane (0.045M in acetone). 11.8 g (99% yield) of the title compound is isolated: mp 84°-91° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05262538 |
| Source dataset | uspto-grants-1993_11 |
| ORD ID | ord-bd28bc9a3f394ae3a460136e6323746f |
| Source note | uspto-grants-1993_11 |