Methyl iodide → 131988-13-1

HRID 257867Notes

Reaction equation

HRID 257867 reaction equation
[CH3:1][I:2].[CH2:3]([O:6][C:7]1[C:8]([C:12]2[CH:13]=[N:14][CH:15]=[CH:16][CH:17]=2)=[N:9][S:10][N:11]=1)[CH2:4][CH3:5]>CC(C)=O>[I-:2].[CH2:3]([O:6][C:7]1[C:8]([C:12]2[CH:13]=[N+:14]([CH3:1])[CH:15]=[CH:16][CH:17]=2)=[N:9][S:10][N:11]=1)[CH2:4][CH3:5]

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 15180132HCID 15180132, compound

Product 1

HCID 15819045131988-13-1

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

A mixture of methyl iodide (0.37 ml, 6 mmol) and 3-(4-propoxy-1,2,5-thiadiazole-3-yl)pyridine (700 mg, 3.1 mmol) in acetone (10 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration to yield 0.98 g (88%)

Workup

  1. customThe title compound precipitated from the solution
  2. filtrationwas collected by filtration
  3. customto yield 0.98 g (88%)

Sources & evidence

ORD record
ord-bf7efa7513004c08ab1591c02e8b1a40
Source dataset
uspto-grants-1993_11
Patent number
US05264444

Reaction notes

Loading…