Methyl iodide → HCID 19075471, compound

HRID 257870Notes

Reaction equation

HRID 257870 reaction equation
[CH3:1][I:2].[CH:3]([O:6][C:7]1[C:8]([C:12]2[CH:13]=[N:14][CH:15]=[CH:16][CH:17]=2)=[N:9][S:10][N:11]=1)([CH3:5])[CH3:4]>CC(C)=O>[I-:2].[CH:3]([O:6][C:7]1[C:8]([C:12]2[CH:13]=[N+:14]([CH3:1])[CH:15]=[CH:16][CH:17]=2)=[N:9][S:10][N:11]=1)([CH3:5])[CH3:4]

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 19016549HCID 19016549, compound

Product 1

HCID 19075471HCID 19075471, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

A mixture of methyl iodide (0.3 ml, 5 mmol) and 3-(4-isopropoxy-1,2,5-thiadiazol-3-yl)pyridine (540 mg, 2.4 mmol) in acetone (5 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration to yield 0.68 g (77%).

Workup

  1. customThe title compound precipitated from the solution
  2. filtrationwas collected by filtration
  3. customto yield 0.68 g (77%)

Sources & evidence

ORD record
ord-a353b81da9b94ecc810ed6d4d34d95c5
Source dataset
uspto-grants-1993_11
Patent number
US05264444

Reaction notes

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