Methyl iodide → HCID 19075414, compound

HRID 257874Notes

Reaction equation

HRID 257874 reaction equation
[CH3:1][I:2].[CH2:3]([O:7][C:8]1[C:9]([C:13]2[CH:14]=[N:15][CH:16]=[CH:17][CH:18]=2)=[N:10][S:11][N:12]=1)[CH:4]([CH3:6])[CH3:5]>CC(C)=O>[I-:2].[CH2:3]([O:7][C:8]1[C:9]([C:13]2[CH:14]=[N+:15]([CH3:1])[CH:16]=[CH:17][CH:18]=2)=[N:10][S:11][N:12]=1)[CH:4]([CH3:6])[CH3:5]

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 19075496HCID 19075496, compound

Product 1

HCID 19075414HCID 19075414, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

A mixture of methyl iodide (0.6 ml, 10 mmol) and 3-(4-isobutoxy-1,2,5-thiadiazol-3-yl)pyridine (588 mg, 2.5 mmol) in acetone (5 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration to yield 0.88 g (87%).

Workup

  1. customThe title compound precipitated from the solution
  2. filtrationwas collected by filtration
  3. customto yield 0.88 g (87%)

Sources & evidence

ORD record
ord-4609cebac4894fab802f68d59233f4d8
Source dataset
uspto-grants-1993_11
Patent number
US05264444

Reaction notes

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