Methyl iodide → HCID 19075288, compound

HRID 257880Notes

Reaction equation

HRID 257880 reaction equation
[CH3:1][I:2].[CH2:3]([O:10][C:11]1[C:12]([C:16]2[CH:17]=[N:18][CH:19]=[CH:20][CH:21]=2)=[N:13][S:14][N:15]=1)[C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1>CC(C)=O>[I-:2].[CH2:3]([O:10][C:11]1[C:12]([C:16]2[CH:17]=[N+:18]([CH3:1])[CH:19]=[CH:20][CH:21]=2)=[N:13][S:14][N:15]=1)[C:4]1[CH:5]=[CH:6][CH:7]=[CH:8][CH:9]=1

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 19075281HCID 19075281, compound

Product 1

HCID 19075288HCID 19075288, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

A mixture of methyl iodide (0.5 ml, 7.5 mmol) and 3-(4-benzyloxy-1,2,5-thiadiazol-3-yl)pyridine (673 mg, 2.5 mmol) in acetone (5 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration to yield 0.75 g (73%).

Workup

  1. customThe title compound precipitated from the solution
  2. filtrationwas collected by filtration
  3. customto yield 0.75 g (73%)

Sources & evidence

ORD record
ord-cf1596310cc749bfa557efd21e0d03b0
Source dataset
uspto-grants-1993_11
Patent number
US05264444

Reaction notes

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