Methyl iodide → 3-(3-(4-Pentenyloxy)-1,2,5-thiadiazol-4-yl)-1-methylpyridinium iodide

HRID 257895Notes

Reaction equation

HRID 257895 reaction equation
[CH3:1][I:2].[CH2:3]([O:8][C:9]1[C:10]([C:14]2[CH:15]=[N:16][CH:17]=[CH:18][CH:19]=2)=[N:11][S:12][N:13]=1)[CH2:4][CH2:5][CH:6]=[CH2:7]>CC(C)=O>[I-:2].[CH2:3]([O:8][C:9]1[C:10]([C:14]2[CH:15]=[N+:16]([CH3:1])[CH:17]=[CH:18][CH:19]=2)=[N:11][S:12][N:13]=1)[CH2:4][CH2:5][CH:6]=[CH2:7]

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 190753593-(3-(4-Pentenyloxy)-1,2,5-thiadiazol-4-yl)pyridine

Product 1

HCID 190752153-(3-(4-Pentenyloxy)-1,2,5-thiadiazol-4-yl)-1-methylpyridinium iodide

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

A mixture of methyl iodide (0.5 ml, 7.5 mmol) and 3-(4-(4-pentenyloxy)-1,2,5-thiadiazol-3-yl)pyridine (2.5 mmol) in acetone (10 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration to yield 0.67 g (69%).

Workup

  1. customThe title compound precipitated from the solution
  2. filtrationwas collected by filtration
  3. customto yield 0.67 g (69%)

Sources & evidence

ORD record
ord-9199a46939dc4835a93de3bb9dde9c1a
Source dataset
uspto-grants-1993_11
Patent number
US05264444

Reaction notes

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