Methyl iodide → HCID 19075453, compound

HRID 257897Notes

Reaction equation

HRID 257897 reaction equation
[CH3:1][I:2].[CH2:3]([O:6][C:7]1[C:8]([C:12]2[CH:13]=[N:14][CH:15]=[CH:16][CH:17]=2)=[N:9][S:10][N:11]=1)[CH:4]=[CH2:5]>CC(C)=O>[I-:2].[CH2:3]([O:6][C:7]1[C:8]([C:12]2[CH:13]=[N+:14]([CH3:1])[CH:15]=[CH:16][CH:17]=2)=[N:9][S:10][N:11]=1)[CH:4]=[CH2:5]

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 19075381HCID 19075381, compound

Product 1

HCID 19075453HCID 19075453, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

A mixture of methyl iodide (0.4 ml, 6 mmol) and 3-(4-(2-propenyloxy)-1,2,5-thiadiazol-3-yl)pyridine (3 mmol) in acetone (5 ml) was stirred at room temperature for 18 h. The title compound precipitiated from the solution and was collected by filtration to give 0.96 g (88%).

Workup

  1. filtrationThe title compound precipitiated from the solution and was collected by filtration
  2. customto give 0.96 g (88%)

Sources & evidence

ORD record
ord-cf27e054dfa34943b94e5c48081f095e
Source dataset
uspto-grants-1993_11
Patent number
US05264444

Reaction notes

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