HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hexylamine → HCID 15180169, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hexylamine | HCID 8102 | — |
| Reactant | 3-Chloro-4-(pyridin-3-yl)-1,2,5-thiadiazole | HCID 10488164 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 15180169 | HCID 15180169 | — |
Reaction Steps
A solution of 3-(4-chloro-1,2,5-thiadiazol-3-yl)pyridine (0.59 g, 3 mmol) and hexylamine (1.52 g, 15 mmol) in DMSO (5 ml) was heated at 100° C. for 48 h. After evaporation, water was added to the residue and extracted with ether. The combined organic extracts were dried and evaporated to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05264444 |
| Source dataset | uspto-grants-1993_11 |
| ORD ID | ord-f9449910e68c4016b79ba787e607baca |
| Source note | uspto-grants-1993_11 |