Methyl iodide → HCID 19075222, compound

HRID 257946Notes

Reaction equation

HRID 257946 reaction equation
[CH3:1][I:2].[O:3]1[N:7]=[CH:6][C:5]([C:8]2[CH:9]=[N:10][CH:11]=[CH:12][CH:13]=2)=[N:4]1>CC(C)=O>[I-:2].[O:3]1[N:7]=[CH:6][C:5]([C:8]2[CH:9]=[N+:10]([CH3:1])[CH:11]=[CH:12][CH:13]=2)=[N:4]1

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 19075301HCID 19075301, compound

Product 1

HCID 19075222HCID 19075222, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

Methyl iodide (1 ml, 15 mmol) was added to a solution of 3-(1,2,5-oxadiazol-3-yl)pyridine (430 mg, 2.9 mmol) in acetone (20 ml). The reaction mixture was stirred at room temperature for 18 h. The product precipitated from the solution and the title compound was collected by filtration in 82% (700 mg) yield.

Workup

  1. customThe product precipitated from the solution
  2. filtrationthe title compound was collected by filtration in 82% (700 mg)
  3. customyield

Sources & evidence

ORD record
ord-1fc4b02f923341cb899cd3780f73a941
Source dataset
uspto-grants-1993_11
Patent number
US05264444

Reaction notes

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