Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 1-Butanol | HCID 263 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 15180172 | HCID 15180172 | — |
| Product | HCID 15180173 | HCID 15180173 | — |
Reaction Steps
To a solution of sodium (150 mg, 6.5 mmol) in 1-butanol (5 ml) was added 3-(4-chloro-1,2,5-oxadiazol-3-yl)pyridine (350 mg, 1.9 mmol). The mixture was stirred at 25° C. for 2 h and evaporated. The residue was dissolved in water and extracted with ether. The combined organic phases were dried and evaporated to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05264444 |
|---|
| Source dataset | uspto-grants-1993_11 |
|---|
| ORD ID | ord-c3ea6b93a57d45a8833bc0b5933acd27 |
|---|
| Source note | uspto-grants-1993_11 |
|---|