Methyl iodide → HCID 19075272, compound
Reaction equation
[CH3:1][I:2].[CH2:3]([S:8][C:9]1[C:10]([C:14]2[CH:15]=[N:16][CH:17]=[CH:18][CH:19]=2)=[N:11][S:12][N:13]=1)[CH2:4][CH2:5][CH2:6][CH3:7]>>[I-:2].[CH2:3]([S:8][C:9]1[C:10]([C:14]2[CH:15]=[N+:16]([CH3:1])[CH:17]=[CH:18][CH:19]=2)=[N:11][S:12][N:13]=1)[CH2:4][CH2:5][CH2:6][CH3:7]Participants
3
Procedure
Methyl iodide (0.5 ml, 7.5 mmol) was added to a solution of 3-(4-pentylthio-1,2,5-thiadiazol-3-yl)pyridine (3 mmol) and the reaction mixture was stirred at room temperature for 48 h and evaporated.
Workup
- customevaporated
Sources & evidence
- ORD record
- ord-1b570a3348e444afb5751d118201fb09
- Source dataset
- uspto-grants-1993_11
- Patent number
- US05264444
Reaction notes
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