化工社化工社 化学情報印刷レポート · 研究参考用
Allyl Mercaptan → 4-Allylsulfanylmethyl-2,2-dimethyl-6-thiophen-3-yl-1,2-dihydroquinoline
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Allyl Mercaptan | HCID 13367 | — |
| 反応物 | N-bromobutanimide | HCID 67184 | — |
| 反応物 | 2,2,4-Trimethyl-6-thiophen-3-yl-1,2-dihydroquinoline | HCID 22566532 | — |
| 生成物 | 4-Allylsulfanylmethyl-2,2-dimethyl-6-thiophen-3-yl-1,2-dihydroquinoline | HCID 22566534 | — |
反応手順
2,2,4-Trimethyl-6-thiophen-3-yl-1,2-dihydroquinoline was brominated with NBS using the procedure described in Example 1 and then coupled with allyl mercaptan using the procedure described in Example 2 to provide 22 mg of the title compound as a oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06858627B2 |
| 出典データセット | uspto-grants-2005_02 |
| ORD ID | ord-2ae737324b1e4979a5f2376838cc0e72 |
| 出典メモ | uspto-grants-2005_02 |