HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 67746805, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | HCID 15670483 | HCID 15670483 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 67746805 | HCID 67746805 | — |
Reaction Steps
A solution of (2S,4R)-4-benzyloxycarbonylamino-2-[(Z)-5-methoxycarbonyl-1-pentenyl]-1-(phenylmethyl)pyrrolidine (700 mg) and 30% hydrogen bromide in acetic acid (2 ml) was stirred at room temperature for 2 hours and the solvent was evaporated in vacuo to give (2S,4R)-4-amino-2-[(Z)-5-methoxycarbonyl-1-pentenyl]-1-(phenylmethyl)pyrrolidine hydrobromide (800 mg) as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05264453 |
| Source dataset | uspto-grants-1993_11 |
| ORD ID | ord-5800b1acdda043eb828ce11f2054625d |
| Source note | uspto-grants-1993_11 |