HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromo-3-tert-butylbenzene → (3-tert-Butyl-phenylethynyl)-trimethyl-silane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromo-3-tert-butylbenzene | HCID 343798 | — |
| Reactant | ((4-(tert-Butyl)phenyl)ethynyl)trimethylsilane | HCID 14989664 | — |
| Product | (3-tert-Butyl-phenylethynyl)-trimethyl-silane | HCID 14989665 | — |
Reaction Steps
Using the same general procedure as described for Compound 21, but using 3-tert-butyl-bromobenzene, (Compound 24) the title compound was synthesized as a colorless oil. PMR (CDCl3): & 0.36 (9H, s), 1.40 (9H, s), 7.32 (1H, m), 7.37-7.47 (2H, m), 7.61 (1H, m).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05264456 |
| Source dataset | uspto-grants-1993_11 |
| ORD ID | ord-32841561546241059a0ed804a4358357 |
| Source note | uspto-grants-1993_11 |