참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Formaldehyde | HCID 712 | — |
| 반응물 | Phenol | HCID 996 | — |
| 반응물 | Sulfuric Acid | HCID 1118 | — |
| 반응물 | Diphenyl Ether | HCID 7583 | — |
| 생성물 | Formaldehyde;phenol | HCID 172281 | — |
반응 단계
An apparatus as described in Example 1 was charged with diphenyl ether (0.1 mol), phenol (0.1 mol) and sulfuric acid (0.5 g). The reagents were heated to 80° C. and stirring started. Formaldehyde (13 mL, 0.17 mol) was added dropwise resulting in the rapid formation of a solid product. After the addition was complete, the mixture was heated under reflux for 1 hour. The resulting product was a solid, insoluble mass.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05264500 |
|---|
| 출처 데이터셋 | uspto-grants-1993_11 |
|---|
| ORD ID | ord-a3d8486b5493447fb6d60130f64ea8fc |
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| 출처 메모 | uspto-grants-1993_11 |
|---|
