HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Octanol → Octyl bromoacetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Octanol | HCID 957 | — |
| Reactant | Toluene | HCID 1140 | — |
| Reactant | Bromoacetic Acid | HCID 6227 | — |
| Catalyst | p-Toluenesulfonic acid | HCID 6101 | — |
| Product | Octyl bromoacetate | HCID 347413 | 113.4% |
Reaction Steps
There were added to 150 ml of toluene, 20 g of bromoacetic acid, 20 g of n-octyl alcohol and 2.5 g of p-toluenesulfonic acid, and azeotropical dehydration was carried out for 1.5 hours. After cooling, toluene was distilled off at reduced pressure, and 41 g of n-octyl bromoacetate were obtained by vacuum distillation (110° C., 11 mm Hg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05266453 |
| Source dataset | uspto-grants-1993_11 |
| ORD ID | ord-1dfee39f792048d6a5a26305e468a175 |
| Source note | uspto-grants-1993_11 |