HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Dihydroxybenzaldehyde → HCID 19104790, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Dihydroxybenzaldehyde | HCID 7213 | — |
| Reactant | 2-Chloro-N,N-dimethylethylamine | HCID 7901 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Solvent | Methyl Ethyl Ketone | HCID 6569 | — |
| Product | HCID 19104790 | HCID 19104790 | — |
Reaction Steps
A mixture containing 0.8 mole of 2,4-dihydroxy-benzaldehyde, 0.8 mole of 2-chloro-1-dimethylaminoethane and 1.6 mole of potassium carbonate in 1200 ml of anhydrous methyl ethyl ketone is refluxed for 1 hour 30 minutes with stirring.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05266565 |
| Source dataset | uspto-grants-1993_11 |
| ORD ID | ord-ec72dd08c30d4978b19a3cc3199775e2 |
| Source note | uspto-grants-1993_11 |