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HRID258280

反应详情

EQUATION

反应方程式

HRID 258280 的结构方程式

REACTANTS

反应物

4
结构：OCC(O)CO
HCID753

Glycerol

C3H8O3

结构：O
HCID962

Water

H2O

结构：CC(C)[C@@H]1CC[C@@H](C)CC1=O
HCID26447

未命名化合物

结构：O=S(=O)([O-])O.[K+]
HCID516920

Potassium bisulfate

HKO4S

PRODUCTS

生成物

1
结构：CC(C)[C@@H]1CC[C@@H](C)CC12OCC(CO)O2
HCID9964606

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：Cc1ccccc1
溶剂HCID1140

Toluene

C7H8

PROCEDURE

实验过程

In a 2 l three-necked flask there are introduced 308 g of 1-menthone (2 mol), 276 g of glycerol (3 mol) and 5 g of potassium hydrogen sulphate in toluene. This mixture is refluxed in a water separator. After 7 hours, 42 g of water have separated. The mixture is neutralised and distilled.

WORKUP

后处理

  1. custom42 g of water have separated
  2. distillationdistilled