HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyanuric chloride → Anthraquinone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyanuric chloride | HCID 7954 | — |
| Reactant | HCID 15076661 | HCID 15076661 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | Anthraquinone | HCID 6780 | — |
Reaction Steps
1-Amino-4-(3'-amino-2',4',6'-trimethyl-5'-sulfophenylthio)anthraquinone-2-sulfonic acid (23.7 parts), cyanuric chloride (9.3 parts) and 1-aminobenzene-3-β-sulfatoethylsulfone (14.1 parts) were subjected to condensation reactions one after another in an aqueous medium in a usual manner, followed by a condensation reaction with pyridine (4.5 parts) at 60° to 70° C. under a weak acid condition. Thereafter, salting out of the reaction mixture gave an anthraquinone compound of the following formula (free acid form). ##STR580##
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05266696 |
| Source dataset | uspto-grants-1993_11 |
| ORD ID | ord-032c890d785c4e79b39ef949707e5b8c |
| Source note | uspto-grants-1993_11 |