Aniline → HCID 54078375, compound

HRID 258374Notes

Reaction equation

HRID 258374 reaction equation
[N:1]([C:4](=[CH:10][N:11]([CH3:13])[CH3:12])[C:5]([O:7][CH2:8][CH3:9])=[O:6])=[C:2]=[O:3].[NH2:14][C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1>C1(C)C=CC=CC=1>[C:5]([C:4]([NH:1][C:2]([NH:14][C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1)=[O:3])=[CH:10][N:11]([CH3:12])[CH3:13])([O:7][CH2:8][CH3:9])=[O:6]

Participants

4

Reactant 2

HCID 6115AnilineHCID 54395864HCID 54395864, compound

Product 1

HCID 54078375HCID 54078375, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

To a solution of Ethyl 2-isocyanato-3-(dimethylamino)-propenoate (5.52 g) in toluene (250 mL) was added aniline (2.79 g). The reaction was stirred at room temperature for 30 min. The resulting solid was collected and dried to yield N-(1-Carboethoxy-2-dimethylaminovinyl)-N'-phenyl urea as a white solid.

Workup

  1. customThe resulting solid was collected
  2. customdried

Sources & evidence

ORD record
ord-6bad85d10f594f90aa0cb70d809e3ef4
Source dataset
uspto-grants-1993_11
Patent number
US05266698

Reaction notes

Loading…