HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Iodide → HCID 178502576, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | Phosphinecarboxylic acid, 1,1-diethoxy-, methyl ester, 1-oxide | HCID 170573 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 178502576 | HCID 178502576 | — |
Reaction Steps
A solution of 5.9 parts of diethyl methoxycarbonylphosphonate and 4.5 parts of sodium iodide was stirred at room temperature in 50 parts of tetrahydrofuran for 60 hours. The resulting mixture was filtered to give 3.5 parts of the desired ethyl sodium methoxycarbonylphosphonate, m.p. 123° d.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04033749 |
| Source dataset | uspto-grants-1977_07 |
| ORD ID | ord-7f8fb2dabf104e6b91e11cc6e135581c |
| Source note | uspto-grants-1977_07 |