HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperidine → HCID 20365141, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | 5-(3-Bromopropyl)-2,3-dihydro-1H-indene | HCID 12646177 | — |
| Solvent | Toluene | HCID 1140 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 20365141 | HCID 20365141 | — |
Reaction Steps
The crude 3-(5-Indanyl)-1-bromopropane (13.0 g, 0.054 M) is dissolved in 200 ml toluene and treated with 50 g of piperidine. The mixture is heated under reflux overnight, then cooled and diluted with ether to precipitate salts. The salts are removed by filtration and the solvent removed from the filtrate in vacuo. The residue is distilled collecting 8.4 g (64%) of desired product boiling at 135°-140° (0.15 mm).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04033971 |
| Source dataset | uspto-grants-1977_07 |
| ORD ID | ord-ecf5ce9540a94059a23b52bb29e84cd8 |
| Source note | uspto-grants-1977_07 |