Phenol → HCID 131710834, compound
Reaction equation
[CH2:1]([S:15][CH3:16])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14].[Cl:17]Cl.[C:19]1([OH:25])[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1>>[Cl-:17].[OH:25][C:19]1[CH:24]=[CH:23][C:22]([CH2:14][CH2:13][CH2:12][CH2:11][CH2:10][CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2][CH2:1][SH+:15][CH3:16])=[CH:21][CH:20]=1Participants
4
Procedure
(4-hydroxyphenyl)n-tetradecylmethyl sulfonium chloride was prepared using as reactants n-tetradecylmethyl sulfide, chlorine and phenol according to the general procedure described in French patent 1,377,019. The product has a melting point of 136.2° - 137.2° C. and the structure was confirmed by elemental and NMR analyses.
Sources & evidence
- ORD record
- ord-d14342e49a61450096ca8468b31b2f78
- Source dataset
- uspto-grants-1977_07
- Patent number
- US04034046
Reaction notes
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