Cyclohexylamine → HCID 178479729, compound

HRID 258664Notes

Reaction equation

HRID 258664 reaction equation
[Cl:1][C:2]1[C:19]2[C:14](=[CH:15][CH:16]=[CH:17][CH:18]=2)[N:13]=[C:4]([C:5]([NH:7][C:8]2[NH:12][N:11]=[N:10][N:9]=2)=[O:6])[CH:3]=1.[CH:20]1([NH2:26])[CH2:25][CH2:24][CH2:23][CH2:22][CH2:21]1>O>[ClH:1].[CH:20]1([NH:26][C:2]2[C:19]3[C:14](=[CH:15][CH:16]=[CH:17][CH:18]=3)[N:13]=[C:4]([C:5]([NH:7][C:8]3[NH:12][N:11]=[N:10][N:9]=3)=[O:6])[CH:3]=2)[CH2:25][CH2:24][CH2:23][CH2:22][CH2:21]1

Participants

4

Reactant 2

HCID 7965CyclohexylamineHCID 178522680HCID 178522680, compound

Product 1

HCID 178479729HCID 178479729, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

4-Chloro-N(1H-tetrazol-5-yl)quinaldamide (0.55 g), cyclohexylamine (3 ml) and water (5 ml) were heated on a steam bath for 3 hours and cooled. The solid was collected and dried, m.p. 245° (d).

Workup

  1. temperaturecooled
  2. customThe solid was collected
  3. customdried

Sources & evidence

ORD record
ord-e0a263a6a42746dbb948870d446dadd3
Source dataset
uspto-grants-1977_07
Patent number
US04034075

Reaction notes

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