HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl vinyl ketone → 7-phenylheptane-2,5-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl vinyl ketone | HCID 6570 | — |
| Reactant | Benzenepropanal | HCID 7707 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 7-phenylheptane-2,5-dione | HCID 3263122 | — |
Reaction Steps
67.1 g (0.5 mol) of hydrocinnamaldehyde, 35.1 g (0.5 mol) of methyl vinyl ketone, 13.5 g (0.05 mol) of Cat. 1, 20.2 g (0.2 mol) of triethylamine and 500 ml of ethanol are brought together, in the manner described in Example 1. The product is worked up as described in Example 21. Fractional distillation gives 1-phenyl-heptane-3,6-dione.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04035395 |
| Source dataset | uspto-grants-1977_07 |
| ORD ID | ord-dd04568c0acb4b35a994c6a31e09771c |
| Source note | uspto-grants-1977_07 |