HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → ((2-Aminoethyl)thio)acetic acid, methyl ester, hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 2,2-Dimethoxypropane | HCID 6495 | — |
| Reactant | HCID 4474780 | HCID 4474780 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | ((2-Aminoethyl)thio)acetic acid, methyl ester, hydrochloride | HCID 170337 | — |
Reaction Steps
13.5 g of S-(β-aminoethyl)mercaptoacetic acid and 10.8 g of 2,2-dimethoxy propane are added, successively, to a solution of 7.3 g of gaseous hydrochloric acid in 20 cc of methanol. The solution is permitted to stand for 12 hours at ambient temperature. The flakes formed (17.5 g) are filtered and washed with ethyl acetate. Fusion point = 100° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04035492 |
| Source dataset | uspto-grants-1977_07 |
| ORD ID | ord-80dbc8443be6466a94408aff2a12ece9 |
| Source note | uspto-grants-1977_07 |