HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenacyl bromide → 2-isoquinolinium-2-yl-1-phenylethan-1-one bromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenacyl bromide | HCID 6259 | — |
| Reactant | Isoquinoline | HCID 8405 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 2-isoquinolinium-2-yl-1-phenylethan-1-one bromide | HCID 2794851 | — |
Reaction Steps
A solution of phenacyl bromide (20 g) in dry ether (100 ml) was added, with stirring, to a solution of isoquinoline (13 g) in ether (50 L ml). The solution was stirred for 30 minutes, and allowed to stand overnight. The precipitated product was filtered off, washed well with ether, and dried. Yield 26.8 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04035499 |
| Source dataset | uspto-grants-1977_07 |
| ORD ID | ord-5a2499b814144ed29c3e7df031ffc55d |
| Source note | uspto-grants-1977_07 |