HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(1H-Pyrrol-1-Yl)Phenol → Pyrrolo[2,1-c][1,4]benzoxazine-4-acetic acid ethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(1H-Pyrrol-1-Yl)Phenol | HCID 712334 | — |
| Reactant | Phenol, 4-chloro-2-(1H-pyrrol-1-yl)- | HCID 10058445 | — |
| Reactant | 8-chloro-4-methyl-4H-pyrrolo[2,1-c][1,4]-benzoxazine-4-acetic acid | HCID 12340635 | — |
| Product | Pyrrolo[2,1-c][1,4]benzoxazine-4-acetic acid ethyl ester | HCID 54560571 | — |
Reaction Steps
In the same manner but replacing N-(2-hydroxyphenyl)pyrrole with an equivalent amount of N-(5-chloro-2-hydroxyphenyl)pyrrole, described in Example 1, 8-chloro-4-methyl-4H-pyrrolo[2,1-c][1,4]-benzoxazine-4-acetic acid, νmaxCHCl3 2,900 - 2,500, 1,728, 1,498, 1,445 cm-1, is obtained via the intermediate ester, 8-chloro-4-methyl-4H-, pyrrolo[2,1-c][1,4]benzoxazine-4-acetic acid ethyl ester, νmaxCHCl3 1,732 cm-1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04035495 |
| Source dataset | uspto-grants-1977_07 |
| ORD ID | ord-340c99e13fab4a5491ebe85f9fca6cb2 |
| Source note | uspto-grants-1977_07 |