HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(1H-Pyrrol-1-Yl)Phenol → HCID 12340630, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(1H-Pyrrol-1-Yl)Phenol | HCID 712334 | — |
| Reactant | Phenol, 4-chloro-2-(1H-pyrrol-1-yl)- | HCID 10058445 | — |
| Reactant | 8-chloro-4-methyl-4H-pyrrolo[2,1-c][1,4]benzoxazine-4-carboxylic acid | HCID 12340633 | — |
| Product | HCID 12340630 | HCID 12340630 | — |
Reaction Steps
In the same manner but replacing N-(2-hydroxyphenyl)-pyrrole with an equivalent amount of N-(5-chloro-2-hydroxyphenyl)-pyrrole, 8-chloro-4-methyl-4H-pyrrolo[2,1-c][1,4]benzoxazine-4-carboxylic acid, m.p. 153° - 154° C (dec), νmaxCHCl3 1,725, 1,510, 1,330cm-1, is obtained via the intermediate ester, 8-chloro-4-methyl-4H-pyrrolo-[2,1-c][1,4]benzoxazine-4-carboxylic acid ethyl ester, νmaxCHCl3 1,735 cm-1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04035495 |
| Source dataset | uspto-grants-1977_07 |
| ORD ID | ord-63e1ff11db8b45b991f848653de7b9fc |
| Source note | uspto-grants-1977_07 |