Formaldehyde → HCID 21423226, compound

HRID 259150Notes

Reaction equation

HRID 259150 reaction equation
[N:1]1([C:6]2[CH:11]=[CH:10][C:9]([SH:12])=[CH:8][CH:7]=2)[CH:5]=[N:4][N:3]=[N:2]1.[CH2:13]=O.[NH:15]1[CH2:20][CH2:19][O:18][CH2:17][CH2:16]1>ClCCl.CCCCCC>[N:1]1([C:6]2[CH:7]=[CH:8][C:9]([S:12][CH2:13][N:15]3[CH2:20][CH2:19][O:18][CH2:17][CH2:16]3)=[CH:10][CH:11]=2)[CH:5]=[N:4][N:3]=[N:2]1

Participants

5

Reactant 3

HCID 712FormaldehydeHCID 8083MorpholineHCID 214232364-(1H-Tetrazol-1-yl)benzene-1-thiol

Product 1

HCID 21423226HCID 21423226, compound

Reagents, catalysts & solvents 1

HCID 21226440Methylenechloride HexaneSolvent

Procedure

Following the general procedure of Example 10, p-(1H-tetrazol-1-yl)benzenethiol is treated with formalin and morpholine to give the 4-[p-(1H-tetrazol-1-yl)phenylthiomethyl]morpholine as white crystals from dichloromethane-hexane, m.p. 118.5°-121° C.

Sources & evidence

ORD record
ord-44c713dd1cf54cd6ad2f821d02b63003
Source dataset
uspto-grants-1977_07
Patent number
US04036849

Reaction notes

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