HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 259163Generated: October 31, 2026
Aniline → 2,3-Dibromo-N-(phenylcarbamoyl)propanamide
https://huagongshe.com/reaction/259163
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | 2,3-Dibromopropanoyl isocyanate | HCID 20318538 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | 2,3-Dibromo-N-(phenylcarbamoyl)propanamide | HCID 20318540 | — |
Reaction Steps
9.5 g of aniline are dissolved in 100 ml of anhydrous benzene and a solution of 26.0 g of 2,3-dibromopropionyl isocyanate in 100 ml of benzene is added dropwise with cooling at 10 to 15° C. After stirring for 2 hours, the crystal sludge is diluted with the same volume of petroleum ether, filtered, washed with petroleum ether and dried. Yield: 30.0 g, m.p: 160°-161° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04036850 |
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| Source dataset | uspto-grants-1977_07 |
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| ORD ID | ord-280ea10ba53740659e5917008497853f |
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| Source note | uspto-grants-1977_07 |
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