HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-Cresol → HCID 23678654, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-Cresol | HCID 335 | — |
| Reactant | 2-Ethylhexanol | HCID 7720 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | HCID 23678654 | HCID 23678654 | — |
Reaction Steps
A five liter flask was equipped with a stirrer, thermometer dropping funnel, heating mantle, Dean-Stark trap and a reflux condenser. 329 grams of a 48.6% aqueous solution of NaOH was added to the flask along with 2000 ml of a 4:1 mixture of xylene and 2-ethyl-1-hexanol. 433 grams of commercial cresol (99.4% pure) was slowly added. The batch was heated to reflux to collect the water. The product was a solution of sodium cresolate:xylene-2-ethyl-1-hexanol mixture.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04036873 |
| Source dataset | uspto-grants-1977_07 |
| ORD ID | ord-ac8d835ce0494dc0b3c5f923698ddb39 |
| Source note | uspto-grants-1977_07 |