HuagongsheHuagongshe Chemistry Print Report · For research reference only
m,alpha-Dichlorotoluene → HCID 23432657, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m,alpha-Dichlorotoluene | HCID 12103 | — |
| Reactant | Potassium thiocyanate | HCID 516872 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 23432657 | HCID 23432657 | — |
Reaction Steps
The mixture of 250 g of m-chlorobenzyl chloride, 16.6 g of potassium thiocyanate and 150 ml of 95% aqueous ethanol is refluxed for 3 hours and evaporated. The residue is taken up in methylene chloride and water, the organic solution separated; washed with water dried and evaporated to yield the m-chlorobenzyl-thiocyanate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04036965 |
| Source dataset | uspto-grants-1977_07 |
| ORD ID | ord-df394d2d42e642ce9d8ae2c704cc6528 |
| Source note | uspto-grants-1977_07 |