Water ethanol → HCID 86733846, compound

HRID 259258Notes

Reaction equation

HRID 259258 reaction equation
[CH2:1]([OH:3])[CH3:2].[OH2:4].[C:5]([C:8]1[CH:16]=[C:15]([CH3:17])[C:14]([CH3:18])=[CH:13][C:9]=1[C:10]([OH:12])=[O:11])(=O)[CH3:6]>O>[OH2:3].[CH3:6][C:5]1[C:8]2[C:9](=[CH:13][C:14]([CH3:18])=[C:15]([CH3:17])[CH:16]=2)[C:10](=[O:11])[O:12][C:2]=1[C:1]([OH:4])=[O:3]

Participants

4

Reactant 2

HCID 19096565Water ethanolHCID 23423454HCID 23423454, compound

Product 1

HCID 86733846HCID 86733846, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

4,6,7- Trimethylisocoumarin -3- carboxylic acid monohydrate, mp. (EtOH-H2O) 241°, (Found: C, 62.27; H, 5.74. C13H12O4. H2O requires C, 62.39; H, 5.64) was prepared from 2- acetyl -4, 5- dimethyl benzoic acid by an analogous procedure to that described in Example 2.

Sources & evidence

ORD record
ord-39507d4e44e9433090316a317fa31aa5
Source dataset
uspto-grants-1977_07
Patent number
US04036964

Reaction notes

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