HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 21162245, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 15566017 | HCID 15566017 | — |
| Product | HCID 21162245 | HCID 21162245 | — |
Reaction Steps
Dry hydrogen chloride was passed into a solution of N,N'-bis-[2-((5-methyl-4-imidazolyl)methylthio)ethyl]thiourea (7.7 g) in methanol at 80° for 5 hours. Concentration and re-evaporation with isopropyl alcohol afforded S-methyl-N,N'-bis-[2-((5-methyl-4-imidazolyl)methylthio)ethyl ]isothiourea trihydrochloride (9.0 g), m.p. 212°-215° (isopropyl alcohol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04036971 |
| Source dataset | uspto-grants-1977_07 |
| ORD ID | ord-b07e4dc03e4147daba1b279ef9aab5ef |
| Source note | uspto-grants-1977_07 |