HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 135580970, compound → HCID 178433677, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 135580970 | HCID 135580970 | — |
| Reactant | HCID 178433288 | HCID 178433288 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178433677 | HCID 178433677 | — |
Reaction Steps
4-Cyanothiophenol was treated with hydrogen chloride in ether at 0° and the hydrochloride salt produced was treated with potassium carbonate to give ethyl 4-mercaptobenzimidate. Ethyl 4-mercaptobenzimidate was treated with 4-methyl-5-[(2-aminoethyl)thiomethyl]imidazole in dry ethanol at room temperature to give the title product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04036971 |
| Source dataset | uspto-grants-1977_07 |
| ORD ID | ord-d847de52e3a4415fb15a5116e8721e07 |
| Source note | uspto-grants-1977_07 |