HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenyl Isothiocyanate → HCID 12939879, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenyl Isothiocyanate | HCID 7673 | — |
| Reactant | N-[(4-Bromophenyl)methyl]propan-2-amine | HCID 12939866 | — |
| Product | HCID 12939879 | HCID 12939879 | 88% |
Reaction Steps
Following the procedure described in Example 1, process variant (a), 23 g of N-(4-bromobenzyl)-N-isopropylamine were reacted with 14 g of phenyl isothiocyanate. 32 g of N-(4-bromobenzyl)-N-isopropyl-N'-phenylthiourea were obtained. Yield: 88%. Melting point: 133.5°-134.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04036986 |
| Source dataset | uspto-grants-1977_07 |
| ORD ID | ord-05a6e7f3fd2d40379bbe6e598ce0085c |
| Source note | uspto-grants-1977_07 |