HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine → N-(4,5,6,7-tetrahydrobenzo[b]thien-4-yl)-4-morpholinecarboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | 4-Isocyanato-4,5,6,7-tetrahydro-1-benzothiophene | HCID 20537301 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | N-(4,5,6,7-tetrahydrobenzo[b]thien-4-yl)-4-morpholinecarboxamide | HCID 20348898 | — |
Reaction Steps
In the manner outlined in Example 6, except for using diethyl ether instead of methylene chloride, 4,5,6,7-tetrahydrobenzo[b]thien-4-yl isocyanate is allowed to react with morpholine to give N-(4,5,6,7-tetrahydrobenzo[b]thien-4-yl)-4-morpholinecarboxamide, which melts at 152° C. to 154° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04036979 |
| Source dataset | uspto-grants-1977_07 |
| ORD ID | ord-b96acfb582c947279189dea53382f095 |
| Source note | uspto-grants-1977_07 |