HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol hydrochloride → 4,5,6,7-Tetrahydro-7-oxobenzo[b]thiophen-4-amine hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol hydrochloride | HCID 21887872 | — |
| Reactant | N-(7-Oxo-4,5,6,7-tetrahydro-1-benzothiophen-4-yl)formamide | HCID 23347790 | — |
| Product | 4,5,6,7-Tetrahydro-7-oxobenzo[b]thiophen-4-amine hydrochloride | HCID 23347795 | — |
Reaction Steps
In the manner described in Example 36, N-formyl-4,5,6,7-tetrahydro-7-oxobenzo[b]thiophen-4-amine is hydrolyzed with 2N hydrochloric acid/ethanol to afford 4,5,6,7-tetrahydro-7-oxobenzo[b]thiophen-4-amine hydrochloride, melting point 230° C. to 232° C. (dec.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04036979 |
| Source dataset | uspto-grants-1977_07 |
| ORD ID | ord-f3b71ccd774640f6a90e98c3f68fcd17 |
| Source note | uspto-grants-1977_07 |