HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloral → Phenyl[4-phenyl-2-(trichloromethyl)-1,3-dioxolan-4-yl]methanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloral | HCID 6407 | — |
| Reactant | 2,3-Dihydroxy-1,2-diphenylpropan-1-one | HCID 85806 | — |
| Product | Phenyl[4-phenyl-2-(trichloromethyl)-1,3-dioxolan-4-yl]methanone | HCID 19035357 | 63% |
Reaction Steps
The procedure of Example 1 was repeated except that the starting materials were α-methylolbenzoin and chloral. The product was a 63% yield of 2-trichloromethyl-4-benzoyl-4-phenyl-1, 3-dioxolane, analyzed as follows:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04037021 |
| Source dataset | uspto-grants-1977_07 |
| ORD ID | ord-5c9f0aefb46c431589dc8b79f69e83b0 |
| Source note | uspto-grants-1977_07 |