HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl cyanoacetate → 2-cyano-N-hexylacetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl cyanoacetate | HCID 7764 | — |
| Reactant | Hexylamine | HCID 8102 | — |
| Solvent | 2-Methoxyethanol | HCID 8019 | — |
| Product | 2-cyano-N-hexylacetamide | HCID 4379529 | — |
Reaction Steps
Ethyl cyanoacetate (113 g., 1.0 mole), n-hexylamine (101 g., 1.0 mole) and methyl cellosolve (200 ml.) are refluxed with stirring for 1.5 hours and the solvent is removed under reduced pressure to give N-(n-hexyl) cyanoacetamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04038065 |
| Source dataset | uspto-grants-1977_07 |
| ORD ID | ord-2fb6d6c065f3425996d72127186ff8f2 |
| Source note | uspto-grants-1977_07 |